Pulsed Third-Spin-Assisted Recoupling NMR for Obtaining Long-Range 13C–13C and 15N–13C Distance Restraints
نویسندگان
چکیده
منابع مشابه
Compensated second-order recoupling: application to third spin assisted recoupling.
We consider the effect of phase shifts in the context of second-order recoupling techniques in solid-state NMR. Notably we highlight conditions leading to significant improvements for the Third Spin Assisted Recoupling (TSAR) mechanism and demonstrate the benefits of resulting techniques for detecting long-distance transfer in biomolecular systems. The modified pulse sequences of PAR and PAIN-C...
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ژورنال
عنوان ژورنال: The Journal of Physical Chemistry B
سال: 2020
ISSN: 1520-6106,1520-5207
DOI: 10.1021/acs.jpcb.0c04574